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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2357421Generated: October 30, 2026

Sodium Bicarbonate → HCID 277395, compound

https://huagongshe.com/reaction/2357421

Reaction equation

Participants

RoleNameHCIDCharge
ReactantSodium BicarbonateHCID 516892—
Reactantα-[(4-Hydroxy-3-methoxyphenyl)methylene]benzeneacetic acidHCID 53411296—
ProductHCID 277395HCID 27739572%

Reaction Steps

A mixture of α-phenyl-4-hydroxy-3-methoxy cinnamic acid (0.0083 mol), NaHCO3 (10%, 5 mL) and polyethylene glycol (5 mL) were taken in a 100 ml round bottom flask fitted with a condenser. The flask was shaken well and placed inside the microwave oven and irradiated (200 W, 180° C.) for 10 minutes in parts. After completion of reaction, the reaction mixture was worked (yield 72%) as in example I. Spectral data as given in example I.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS07759527B2
Source datasetuspto-grants-2010_07
ORD IDord-d5e4ef01530649c48224917d5dfd92e5
Source noteuspto-grants-2010_07