HCID 68454064, compound → HCID 68454726, compound

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Reaction Steps

A mixture of N-cyclopropyl-4-methyl-3-(1-(piperidin-4-yl)phthalazin-6-yl)benzamide N-cyclopropyl-4-methyl-3-(1-(piperidin-4-yl)phthalazin-6-yl)benzamide (29 μmol) in 2 mL ethanol was stirred at RT and treated with 2-trifluoromethylamine diacetate (142 μmol). The mixture was stirred at RT for 4 h, then purified directly by silica gel chromatography, eluting with 5% 2 M ammonia methanol/dichloromethane to give the title compound.

Provenance & Evidence