HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2357633Generated: October 31, 2026
1-(Methylsulfonyl)piperazine → HCID 68452804, compound
https://huagongshe.com/reaction/2357633
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | 1-(Methylsulfonyl)piperazine | HCID 709161 | — |
| Reactant | 6-Bromo-1-chlorophthalazine | HCID 22030424 | — |
| Solvent | Dichloromethane methanol | HCID 21226129 | — |
| Product | HCID 68452804 | HCID 68452804 | — |
Reaction Steps
6-Bromo-1-chlorophthalazine (18 mg, 74 umol) and 1-(methylsulfonyl)piperazine (91 mg, 554 μmol) were dissolved in dichloromethane/methanol when the reaction mixture was concentrated by evaporation under a nitrogen line. The concentrate was heated to 120° C. for 6 h to give the title compound. MS (ES+): 373 (M+H)+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patent number | US07759337B2 |
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| Source dataset | uspto-grants-2010_07 |
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| ORD ID | ord-59f013caca3947f5974040eff5713283 |
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| Source note | uspto-grants-2010_07 |
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