Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Methanol | HCID 887 | — |
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Reactant | HCID 178425877 | HCID 178425877 | — |
| Product | HCID 178497700 | HCID 178497700 | — |
Reaction Steps
3-(1-Hydroxyphthalazin-6-yl)-4-methylbenzoic acid (2.71 g, 9.67 mmol) was suspended in methanol (96.7 mL), thionyl chloride (2.12 mL, 29.0 mmol) was added and the mixture was stirred at 50° C. for 1.5 h and at RT overnight. The mixture was concentrated to give the title compound. MS (ES+): 295(M+H)+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US07759337B2 |
|---|
| Source dataset | uspto-grants-2010_07 |
|---|
| ORD ID | ord-026ba7a5091345a19e969aeee4fc0e49 |
|---|
| Source note | uspto-grants-2010_07 |
|---|
