Hydrochloric Acid → HCID 58897789, compound

Participants

Reaction Steps

A mixture of 21.3 g (49.5 mmol) of crude bis(1-methoxy-2-methyl-2,3-dihydro-1H-inden-4-yl)(phenyl)phosphine, 100 ml of 16 M HCl, and 150 ml of methanol was refluxed for 5 hours. This mixture was cooled to ambient temperature, and 100 ml of water was added. The white precipitate that formed was filtered off and dried in vacuum. Yield, 15.0 g (82%) of a white solid.

Provenance & Evidence