HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2357944Generated: November 1, 2026
HCID 59389336, compound → HCID 59389321, compound
https://huagongshe.com/reaction/2357944
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | HCID 59389336 | HCID 59389336 | — |
| Catalyst | HCID 178418406 | HCID 178418406 | — |
| Solvent | Chloroform | HCID 6212 | — |
| Product | HCID 59389321 | HCID 59389321 | 96.4% |
Reaction Steps
Activated manganese dioxide (20.0 g) was added to a solution of the compound of Example 326 (6.00 g) in chloroform (120 mL). The reaction mixture was stirred at 50° C. for 5 hours. Subsequently, the mixture was filtered through Celite. The filtrate was concentrated to afford the title compound as a pale yellow powder (5.74 g).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patent number | US07763617B2 |
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| Source dataset | uspto-grants-2010_07 |
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| ORD ID | ord-e8fb9fb736c44da28e5a8e133c142576 |
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| Source note | uspto-grants-2010_07 |
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