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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2357944Generated: November 1, 2026

HCID 59389336, compound → HCID 59389321, compound

https://huagongshe.com/reaction/2357944

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 59389336HCID 59389336—
CatalystHCID 178418406HCID 178418406—
SolventChloroformHCID 6212—
ProductHCID 59389321HCID 5938932196.4%

Reaction Conditions

Temperature50 °C

Reaction Steps

Activated manganese dioxide (20.0 g) was added to a solution of the compound of Example 326 (6.00 g) in chloroform (120 mL). The reaction mixture was stirred at 50° C. for 5 hours. Subsequently, the mixture was filtered through Celite. The filtrate was concentrated to afford the title compound as a pale yellow powder (5.74 g).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS07763617B2
Source datasetuspto-grants-2010_07
ORD IDord-e8fb9fb736c44da28e5a8e133c142576
Source noteuspto-grants-2010_07