Hydroxyamine hydrochloride → HCID 136013274, compound

Participants

Reaction Steps

The compound of Example 237 (24.0 mg) was dissolved in methanol (3 mL). To this solution, sodium acetate (41.3 mg) and hydroxylamine hydrochloride (17.5 mg) were added at room temperature and the reaction mixture was stirred for 20 min. The solvent was evaporated under reduced pressure and water was added to the residue. The mixture was filtered to afford the title compound as a white powder (15.3 mg, a mixture of E-form and Z-form (E:Z=1:5)).

Provenance & Evidence