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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2357955Generated: October 31, 2026

HCID 59389290, compound → HCID 59389347, compound

https://huagongshe.com/reaction/2357955

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 59389290HCID 59389290—
CatalystHCID 178418406HCID 178418406—
SolventChloroformHCID 6212—
ProductHCID 59389347HCID 5938934797.5%

Reaction Conditions

Temperature50 °C

Reaction Steps

Activated manganese dioxide (3.75 g) was added to a solution of the compound of Example 353 (1.28 g) in chloroform (50 mL). The mixture was stirred at 50° C. for 4 hours. Subsequently, the mixture was filtered through Celite and the filtrate was concentrated to afford the title compound as a colorless powder (1.24 g).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS07763617B2
Source datasetuspto-grants-2010_07
ORD IDord-9921fcbb7d03473198d993a305a6919d
Source noteuspto-grants-2010_07