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HRID2358082

反应详情

EQUATION

反应方程式

HRID 2358082 的结构方程式

REACTANTS

反应物

3
结构：O=C([O-])[O-].[K+].[K+]
HCID11430

Potassium Carbonate

CK2O3

结构：OCCI
HCID12225

Ethanol, 2-iodo-

C2H5IO

结构：O=S(=O)(c1cccc(C2CCNCC2)c1F)C(F)(F)F
HCID57448051

未命名化合物

PRODUCTS

生成物

1
结构：O=S(=O)(c1cccc(C2CCN(CCO)CC2)c1F)C(F)(F)F
HCID67533685

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：CC#N
溶剂HCID6342

Acetonitrile

C2H3N

PROCEDURE

实验过程

Preparation according to Example 1: 4-{2-fluoro-3-[(trifluoromethyl)sulfonyl]phenyl}-piperidine (0.01 g), acetonitrile (2 ml), potassium carbonate (0.01 g) and 2-iodoethanol (0.01 g). MS m/z (rel. intensity, 70 eV) 355 (M+, 1), 325 (15), 324 (bp), 191 (36), 133 (12).

WORKUP

后处理

  1. customPreparation