huagongshe.com
HRID2358083

反应详情

EQUATION

反应方程式

HRID 2358083 的结构方程式

REACTANTS

反应物

3
结构：CI
HCID6328

Methyl iodide

CH3I

结构：O=C([O-])[O-].[K+].[K+]
HCID11430

Potassium Carbonate

CK2O3

结构：O=S(=O)(c1cccc(C2CCNCC2)c1F)C(F)(F)F
HCID57448051

未命名化合物

PRODUCTS

生成物

1
结构：CN1CCC(c2cccc(S(=O)(=O)C(F)(F)F)c2F)CC1
HCID86085874

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：CC#N
溶剂HCID6342

Acetonitrile

C2H3N

PROCEDURE

实验过程

Preparation according to Example 18: 4-{2-fluoro-3-[(trifluoromethyl)sulfonyl]phenyl}-piperidine (0.01 g), acetonitrile (2 ml), potassium carbonate (0.01 g) and iodomethane (0.01 g). MS m/z (rel. intensity, 70 eV) 325 (M+, 63), 324 (bp), 305 (13), 191 (32), 133 (24).

WORKUP

后处理

  1. customPreparation