HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 67533082, compound → HCID 57448065, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 67533082 | HCID 67533082 | — |
| Solvent | Trifluoroacetic acid | HCID 6422 | — |
| Product | HCID 57448065 | HCID 57448065 | — |
Reaction Steps
Preparation according to preparation 2: Tert-butyl 4-[2-fluoro-3-(methylthio)-phenyl]-4-hydroxy-piperidine-1-carboxylate (2.0 g, 5.86 mmol), trifluoroacetic acid (20 ml). Yield: 1.42 g. MS m/z (rel. intensity, 70 eV) 223 (M+, bp), 222 (32), 147 (61), 146 (47), 133 (27).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07763639B2 |
| Source dataset | uspto-grants-2010_07 |
| ORD ID | ord-4aa1ad7356fe4a7dbfca4c236d755b37 |
| Source note | uspto-grants-2010_07 |