HuagongsheHuagongshe Chemistry Print Report · For research reference only
Water → HCID 57448069, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Water | HCID 962 | — |
| Reactant | Carbon Tetrachloride | HCID 5943 | — |
| Reactant | Acetonitrile | HCID 6342 | — |
| Reactant | Sodium periodate | HCID 23667635 | — |
| Reactant | HCID 57448068 | HCID 57448068 | — |
| Catalyst | Ruthenium trichloride | HCID 61850 | — |
| Product | HCID 57448069 | HCID 57448069 | — |
Reaction Steps
Preparation according to preparation 4: 1-bromo-2-fluoro-3-[(trifluoromethyl)thio]benzene (0.37 g), carbon tetrachloride (4 ml), acetonitrile (4 ml), water (8 ml), sodium periodate (0.86 g), ruthenium trichloride (1 mg). Yield: 0.3 g. MS m/z (rel. intensity, 70 eV) 308 (M+, 18), 306 (M+, 19), 239 (57), 173 (60), 94 (bp).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07763639B2 |
| Source dataset | uspto-grants-2010_07 |
| ORD ID | ord-0bd85fb939b4404d816b2e96ead9eec3 |
| Source note | uspto-grants-2010_07 |