HuagongsheHuagongshe Chemistry Print Report · For research reference only
Iodoethane → HCID 67533166, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Iodoethane | HCID 6340 | — |
| Reactant | Sodium borohydride | HCID 4311764 | — |
| Reactant | HCID 57448072 | HCID 57448072 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 67533166 | HCID 67533166 | — |
Reaction Steps
Preparation according to preparation 6: 4-[2-fluoro-3-(2-methyl-1,3-dioxolan-2-yl)phenyl]pyridine (0.95 g, 3.66 mmol), 1-iodoethane (4 ml), ethanol (40 ml), sodium borohydride (1.0 g, 29.3 mmol). Yield: 0.88 g. MS m/z (rel. intensity, 70 eV) 291 (M+, bp), 276 (94), 219 (29), 110 (46), 87 (29).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07763639B2 |
| Source dataset | uspto-grants-2010_07 |
| ORD ID | ord-bf389f5036914b9f965267f2df9d4768 |
| Source note | uspto-grants-2010_07 |