HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 67532664, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | Ethanone, 2,2,2-trifluoro-1-[2-fluoro-3-(4-pyridinyl)phenyl]- | HCID 57448077 | — |
| Catalyst | Platinum oxide (PtO) | HCID 82844 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 67532664 | HCID 67532664 | — |
Reaction Steps
Preparation according to preparation 9: 2,2,2-trifluoro-1-(2-fluoro-3-pyridin-4-ylphenyl)ethanone (1.26 g, 4.68 mmol), hydrochloric acid (0.2 ml, conc), methanol (20 ml), platinum oxide (0.12 g). Yield: 0.98 g. MS m/z (relative intensity, 70 eV) 275 (M+, 94), 274 (66), 149 (23), 101 (25) 56 (bp).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07763639B2 |
| Source dataset | uspto-grants-2010_07 |
| ORD ID | ord-21c8edf354854b9eadd5076346ef6536 |
| Source note | uspto-grants-2010_07 |