HuagongsheHuagongshe Chemistry Print Report · For research reference only
5-Benzothiazolamine, 2-methyl- → HCID 15984148, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 5-Benzothiazolamine, 2-methyl- | HCID 36229 | — |
| Reactant | Ethyl 1-[(3-fluorophenyl)methyl]-5-(trifluoromethyl)-1H-pyrrolo[2,3-b]pyridine-2-carboxylate | HCID 66905320 | — |
| Product | HCID 15984148 | HCID 15984148 | 73.1% |
Reaction Steps
The process is performed according to the method described in step 13.5 of Example 13, starting with 0.35 g (0.96 mmol) of ethyl 5-trifluoromethyl-1-[(3-fluorophenyl)methyl]-1H-pyrrolo[2,3-b]pyridine-2-carboxylate (Example 13.4) and 0.17 g (1.06 mmol) of 5-amino-2-methylbenzothiazole. 0.34 g of expected compound is isolated.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07763636B2 |
| Source dataset | uspto-grants-2010_07 |
| ORD ID | ord-fe5d8f915fdb46b58b65b504753f2f05 |
| Source note | uspto-grants-2010_07 |