HuagongsheHuagongshe Chemistry Print Report · For research reference only
1,2-Dimethyl-1H-benzimidazol-5-amine → HCID 15984952, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1,2-Dimethyl-1H-benzimidazol-5-amine | HCID 965355 | — |
| Reactant | HCID 67546418 | HCID 67546418 | — |
| Product | HCID 15984952 | HCID 15984952 | 51.2% |
Reaction Steps
The process is performed according to the method described in step 2.4 of Example 2, starting with 0.3 g (0.95 mmol) of ethyl 5-fluoro-1-[(3-fluorophenyl)methyl]-1H-pyrrolo[2,3-c]pyridine-2-carboxylate (Example 2.3) and 0.183 g (1.14 mmol) of 5-amino-1,2-dimethylbenzimidazole. 0.21 g of expected compound is isolated.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07763636B2 |
| Source dataset | uspto-grants-2010_07 |
| ORD ID | ord-862649cc2a3b44f6bac0bf08d0d5a7d9 |
| Source note | uspto-grants-2010_07 |