HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydroxyacetonitrile → HCID 19094668, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydroxyacetonitrile | HCID 7857 | — |
| Reactant | 2,2-Diethoxyethylamine | HCID 69524 | — |
| Product | HCID 19094668 | HCID 19094668 | — |
Reaction Steps
A mixture of glycolonitrile (8.33 g, 70% solution in water, 0.1 mol) and aminoacetaldehyde diethyl acetal (14.5 mL, 0.1 mol) was heated to reflux for 3 h. After cooling, the mixture was filtered to remove traces of solid and the filtrate then concentrated in vacuo to give the desired product 4.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07763614B2 |
| Source dataset | uspto-grants-2010_07 |
| ORD ID | ord-d07826fe1d8a4a698beb55d360644a52 |
| Source note | uspto-grants-2010_07 |