HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 68732684, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | HCID 68718774 | HCID 68718774 | — |
| Solvent | Ethyl Acetate | HCID 8857 | — |
| Product | HCID 68732684 | HCID 68732684 | — |
Reaction Steps
A solution of 57 (200 mg, 0.423 mmol) in ethyl acetate (100 mL) was cooled in an ice bath and treated with hydrogen chloride gas for 10 min. The resulting solution was stirred 1.5 h and then warmed to room temperature. Evaporation of the solvent in vacuo gave 58 as a white solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07763614B2 |
| Source dataset | uspto-grants-2010_07 |
| ORD ID | ord-07940e76388f43d29e52f4c5ef97a682 |
| Source note | uspto-grants-2010_07 |