Back
HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2358300Generated: November 1, 2026

Potassium Carbonate → HCID 58828539, compound

https://huagongshe.com/reaction/2358300

Reaction equation

Participants

RoleNameHCIDCharge
ReactantPotassium CarbonateHCID 11430—
ReactantBenzene, ((2-bromoethoxy)methyl)-HCID 73833—
ReactantHCID 11393032HCID 11393032—
SolventDimethylformamideHCID 6228—
ProductHCID 58828539HCID 58828539—

Reaction Conditions

Temperature120 °C

Reaction Steps

A mixture of the phenol 62 (80 mg, 0.25 mmol), K2CO3 (104 mg, 0.75 mmol) and benzyloxyethyl bromide (64 mg, 0.3 mmol) in DMF (3 mL) was heated in a microwave reactor at 120° C. for 15 min. The mixture was filtered and directly purified using an automated high pressure chromatography unit.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS07763614B2
Source datasetuspto-grants-2010_07
ORD IDord-2dadb4b3f10e49689798af3c75a5858a
Source noteuspto-grants-2010_07