HuagongsheHuagongshe Chemistry Print Report · For research reference only
Potassium Carbonate → HCID 58828539, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | Benzene, ((2-bromoethoxy)methyl)- | HCID 73833 | — |
| Reactant | HCID 11393032 | HCID 11393032 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 58828539 | HCID 58828539 | — |
Reaction Conditions
| Temperature | 120 °C |
|---|
Reaction Steps
A mixture of the phenol 62 (80 mg, 0.25 mmol), K2CO3 (104 mg, 0.75 mmol) and benzyloxyethyl bromide (64 mg, 0.3 mmol) in DMF (3 mL) was heated in a microwave reactor at 120° C. for 15 min. The mixture was filtered and directly purified using an automated high pressure chromatography unit.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07763614B2 |
| Source dataset | uspto-grants-2010_07 |
| ORD ID | ord-2dadb4b3f10e49689798af3c75a5858a |
| Source note | uspto-grants-2010_07 |