HuagongsheHuagongshe Chemistry Print Report · For research reference only
Trifluoroacetic acid → HCID 57665528, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Trifluoroacetic acid | HCID 6422 | — |
| Reactant | HCID 68455779 | HCID 68455779 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 57665528 | HCID 57665528 | — |
Reaction Steps
(3-fluoro-4-methanesulfonylamino-5-vinyl-benzyl)-carbamic acid t-butyl ester (1 ml) was put into 25 ml round-bottom flask and dissolved in methylenechloride. To the solution was added trifluoroacetic acid (1 ml) and stirred for one night. After confirming the completion of the reaction with TLC, the reaction solution was concentrated under reduced pressure to yield a brown crude liquid (236.7 mg).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07763657B2 |
| Source dataset | uspto-grants-2010_07 |
| ORD ID | ord-b51e80f440ac4c49b7d36a92d704cf26 |
| Source note | uspto-grants-2010_07 |