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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2358372Generated: October 31, 2026

Trifluoroacetic acid → HCID 57665528, compound

https://huagongshe.com/reaction/2358372

Reaction equation

Participants

RoleNameHCIDCharge
ReactantTrifluoroacetic acidHCID 6422—
ReactantHCID 68455779HCID 68455779—
SolventDichloromethaneHCID 6344—
ProductHCID 57665528HCID 57665528—

Reaction Steps

(3-fluoro-4-methanesulfonylamino-5-vinyl-benzyl)-carbamic acid t-butyl ester (1 ml) was put into 25 ml round-bottom flask and dissolved in methylenechloride. To the solution was added trifluoroacetic acid (1 ml) and stirred for one night. After confirming the completion of the reaction with TLC, the reaction solution was concentrated under reduced pressure to yield a brown crude liquid (236.7 mg).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS07763657B2
Source datasetuspto-grants-2010_07
ORD IDord-b51e80f440ac4c49b7d36a92d704cf26
Source noteuspto-grants-2010_07