HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 68456052, compound → HCID 68453767, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 68456052 | HCID 68456052 | — |
| Catalyst | Trifluoroacetic acid | HCID 6422 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 68453767 | HCID 68453767 | 464.2% |
Reaction Steps
(4-Methanesulfonylamino-3-methyl-5-vinylbenzyl)carbamic acid tert-butyl ester (85.9 mg, 0.09 mmol) was dissolved in CH2Cl2. 5˜6 drops of CF3COOH were added. The reaction mixture was stirred for 12 hr. The reaction mixture was concentrated to yield brownish syrup (100.4 mg).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07763657B2 |
| Source dataset | uspto-grants-2010_07 |
| ORD ID | ord-d88bf5b4e4a34bb588b68b8299c0a1f4 |
| Source note | uspto-grants-2010_07 |