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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2358403Generated: October 30, 2026

Hydrochloric Acid → HCID 68455970, compound

https://huagongshe.com/reaction/2358403

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHydrochloric AcidHCID 313—
ReactantSodium HydroxideHCID 14798—
ReactantHCID 68456145HCID 68456145—
SolventMethanolHCID 887—
SolventWaterHCID 962—
ProductHCID 68455970HCID 68455970100%

Reaction Steps

3-(4-tert-butyl-2-isopropylaminophenyl)acrylic acid methyl ester (0.14 mmol, 37.7 mg) and NaOH (0.68 mmol, 27.39 mg) were added in methanol and water. The reaction mixture was stirred for 12 hrs at room temperature. The reaction mixture was acidified with 5% HCl solution. The mixture was concentrated in vacuo to yield a yellow solid (36.56 mg, 100%).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS07763657B2
Source datasetuspto-grants-2010_07
ORD IDord-bd9b241196d74ba59c07b71b2ec756b8
Source noteuspto-grants-2010_07