HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-(4-tert-Butylphenyl)-2-methylprop-2-enoic acid → 3-(4-tert-Butylphenyl)-2-methylpropanoic acid
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-(4-tert-Butylphenyl)-2-methylprop-2-enoic acid | HCID 54367550 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | 3-(4-tert-Butylphenyl)-2-methylpropanoic acid | HCID 106694 | 93.47% |
Reaction Steps
3-(4-tert-butylphenyl)-2-methylacrylic acid (40.9 mg, 0.19 mmol) and 10 wt. % palladium on activated carbon were added in methanol. The reaction mixture was stirred for 5 hrs under H2 gas. The reaction mixture was filtered with Celite. The filterate was concentrated in vacuo to obtain title compound (39.1 mg, 93.47%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07763657B2 |
| Source dataset | uspto-grants-2010_07 |
| ORD ID | ord-8ef4a8f9a6be45418e08ae4eb8b5e5a0 |
| Source note | uspto-grants-2010_07 |