HuagongsheHuagongshe Chemistry Print Report · For research reference only
Trifluoroacetic acid → HCID 68457029, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Trifluoroacetic acid | HCID 6422 | — |
| Reactant | HCID 76587252 | HCID 76587252 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 68457029 | HCID 68457029 | 154.6% |
Reaction Steps
[1-(4-Ethenesulfonylamino-3-vinyl-phenyl)-ethyl]-carbamic acid tert-butyl ester (20.0 mg, 0.04 mmol) and CF3COOH (5 eq, 0.22 mmol, 17.04 μl) were dissolved in methylene chloride. The reaction mixture was stirred for 12 hrs. A reaction mixture was concentrate to yield [1-(4-Ethenesulfonylamino-3-vinyl-phenyl)-ethylamine (15.6 mg, 76%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07763657B2 |
| Source dataset | uspto-grants-2010_07 |
| ORD ID | ord-4a7fd58791064a65b27fa97eb4b8726c |
| Source note | uspto-grants-2010_07 |