Ammonium Chloride → HCID 68458465, compound

HRID 2358653Notes

Reaction equation

HRID 2358653 reaction equation
[N+:1]([C:4]1[CH:5]=[C:6]([NH:17][C:18](=[O:20])[CH3:19])[CH:7]=[CH:8][C:9]=1[S:10][C:11]1[CH:16]=[CH:15][CH:14]=[CH:13][CH:12]=1)([O-])=O.[NH4+].[Cl-]>[Fe]>[NH2:1][C:4]1[CH:5]=[C:6]([NH:17][C:18](=[O:20])[CH3:19])[CH:7]=[CH:8][C:9]=1[S:10][C:11]1[CH:16]=[CH:15][CH:14]=[CH:13][CH:12]=1

Participants

4

Reactant 2

HCID 25517Ammonium ChlorideHCID 68458075HCID 68458075, compound

Product 1

HCID 68458465HCID 68458465, compound

Reagents, catalysts & solvents 1

HCID 23925IronCatalyst

Procedure

A solution of the product of Example 96b was reduced with Fe and NH4Cl following the procedure from Example 237E to give the title compound.

Sources & evidence

ORD record
ord-4a13c521801341e68b5b394e53111f55
Source dataset
uspto-grants-2010_07
Patent number
US07763731B2

Reaction notes

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