HuagongsheHuagongshe Chemistry Print Report · For research reference only
Phosphorus oxychloride → HCID 13773146, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Phosphorus oxychloride | HCID 24813 | — |
| Reactant | HCID 13773137 | HCID 13773137 | — |
| Solvent | Chloroform | HCID 6212 | — |
| Product | HCID 13773146 | HCID 13773146 | 89.2% |
Reaction Steps
12.0 g of ethyl 3-isobutyrylamino-3-(2-furylcarbonyl)propionate, 60 ml of chloroform and 32.7 g of phosphorus oxychloride are treated in the same manner as described in Example 2. 10.0 g of ethyl 2-[2-isopropyl-5-(2-furyl)-4-oxazolyl]acetate are thereby obtained as an oil. Yield: 89.2%
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04642313 |
| Source dataset | uspto-grants-1987_02 |
| ORD ID | ord-d01b574f2b3e490e99aa4f46111ce121 |
| Source note | uspto-grants-1987_02 |