HuagongsheHuagongshe Chemistry Print Report · For research reference only
Oxalyl chloride → HCID 86615502, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Oxalyl chloride | HCID 65578 | — |
| Reactant | 3-(4-Fluoro-2-nitro-phenoxy)-benzoic acid | HCID 61395640 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 86615502 | HCID 86615502 | — |
Reaction Steps
The product from Example 181b (1.6 g, 5.6 mmol) was treated with oxalyl chloride (0.86 g, 6.7 mmol) and catalytic DMF at room temperature for 6 h. The excess oxalyl chloride was removed under vacuum. The residue was chased with benzene to \give the title compound (1.66 g, 94%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07763731B2 |
| Source dataset | uspto-grants-2010_07 |
| ORD ID | ord-89ce06f72a464cb8b92caf7ed5d57535 |
| Source note | uspto-grants-2010_07 |