Acetyl chloride → N-[3-(4-Methyl-2-nitro-phenylsulfanyl)-phenyl]-acetamide

HRID 2358793Notes

Reaction equation

HRID 2358793 reaction equation
[CH3:1][C:2]1[CH:7]=[CH:6][C:5]([S:8][C:9]2[CH:10]=[C:11]([NH2:15])[CH:12]=[CH:13][CH:14]=2)=[C:4]([N+:16]([O-:18])=[O:17])[CH:3]=1.[C:19](Cl)(=[O:21])[CH3:20]>C(Cl)Cl>[CH3:1][C:2]1[CH:7]=[CH:6][C:5]([S:8][C:9]2[CH:10]=[C:11]([NH:15][C:19](=[O:21])[CH3:20])[CH:12]=[CH:13][CH:14]=2)=[C:4]([N+:16]([O-:18])=[O:17])[CH:3]=1

Participants

4

Reactant 2

HCID 6367Acetyl chlorideHCID 684579173-(4-Methyl-2-nitro-phenylsulfanyl)-phenylamine

Product 1

HCID 68459008N-[3-(4-Methyl-2-nitro-phenylsulfanyl)-phenyl]-acetamide

Reagents, catalysts & solvents 1

HCID 6344DichloromethaneSolvent

Procedure

The title compound was prepared using 3-(4-Methyl-2-nitro-phenylsulfanyl)-phenylamine (8.20 g, 31.50 mmol) and acetyl chloride (2.72 g, 34.65 mmol) dissolved in CH2Cl2. This was stirred at room temperature for 2 hrs at which time the title compound was collected by filtration (8.78 g, 92

Workup

  1. customThe title compound was prepared
  2. filtrationwas collected by filtration (8.78 g, 92

Sources & evidence

ORD record
ord-e61a2ce1169b4ff8b66b8751fdbed28d
Source dataset
uspto-grants-2010_07
Patent number
US07763731B2

Reaction notes

Loading…