HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetyl chloride → N-[3-(4-Methyl-2-nitro-phenylsulfanyl)-phenyl]-acetamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetyl chloride | HCID 6367 | — |
| Reactant | 3-(4-Methyl-2-nitro-phenylsulfanyl)-phenylamine | HCID 68457917 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | N-[3-(4-Methyl-2-nitro-phenylsulfanyl)-phenyl]-acetamide | HCID 68459008 | — |
Reaction Steps
The title compound was prepared using 3-(4-Methyl-2-nitro-phenylsulfanyl)-phenylamine (8.20 g, 31.50 mmol) and acetyl chloride (2.72 g, 34.65 mmol) dissolved in CH2Cl2. This was stirred at room temperature for 2 hrs at which time the title compound was collected by filtration (8.78 g, 92
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07763731B2 |
| Source dataset | uspto-grants-2010_07 |
| ORD ID | ord-e61a2ce1169b4ff8b66b8751fdbed28d |
| Source note | uspto-grants-2010_07 |