反应详情

温度

100 °C

A mixture of 3-nitro-4-chloro phenol (1.59 g, 8.97 mmol), 4-acetamidothiophenol (2 g, 10.76 mmol) and cesium carbonate (7.0 g, 21.53 mmol) in DMF (20 mL) was heated 2.5 h at 100° C. The mixture was cooled, poured onto ice and the resulting solid is collected by filtration and dried under vacuum the title compound leaving a yellow solid (2.7 g, 100%).

1. temperatureThe mixture was cooled
2. additionpoured onto ice
3. filtrationthe resulting solid is collected by filtration
4. dry with materialdried under vacuum the title compound