HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethyl bromoacetate → HCID 13773131, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethyl bromoacetate | HCID 7748 | — |
| Reactant | Sodium hydride | HCID 24758 | — |
| Reactant | 4-Chloro-N-[2-(furan-3-yl)-2-oxoethyl]benzamide | HCID 13773122 | — |
| Product | HCID 13773131 | HCID 13773131 | 77.3% |
Reaction Steps
8.3 g of N-(4-chlorobenzoyl)-(3-furylcarbonyl)methylamine, 1.5 g of 61% sodium hydride and 5.8 g of ethyl bromoacetate are treated in the same manner as described in Preparation 1-(2). 8.5 g of ethyl 3-(4-chlorobenzoylamino)-3-(3-furylcarbonyl)propionate are thereby obtained. Yield: 77.3%
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04642313 |
| Source dataset | uspto-grants-1987_02 |
| ORD ID | ord-df81bac86a9f487f9cf97540113d17b7 |
| Source note | uspto-grants-1987_02 |