HuagongsheHuagongshe Chemistry Print Report · For research reference only
p-Anisoyl chloride → N-[2-(Furan-2-yl)-2-oxoethyl]-4-methoxybenzamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | p-Anisoyl chloride | HCID 7477 | — |
| Reactant | Sodium Bicarbonate | HCID 516892 | — |
| Reactant | 2-Amino-1-(furan-2-yl)ethan-1-one--hydrogen chloride (1/1) | HCID 13226138 | — |
| Product | N-[2-(Furan-2-yl)-2-oxoethyl]-4-methoxybenzamide | HCID 13773125 | 85.7% |
Reaction Steps
8.0 g of (2-furylcarbonyl)methylamine hydrochloride, 10.5 g of sodium bicarbonate and 10.1 g of 4-methoxybenzoyl chloride are treated in the same manner as described in Preparation 1-(1). 11.0 g of N-(4-methoxybenzoyl)-(2-furylcarbonyl)methylamine are thereby obtained. Yield: 85.3%
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04642313 |
| Source dataset | uspto-grants-1987_02 |
| ORD ID | ord-83a2138b48e3480a84e1c9e011dca921 |
| Source note | uspto-grants-1987_02 |