HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethyl bromoacetate → HCID 13773135, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethyl bromoacetate | HCID 7748 | — |
| Reactant | Sodium hydride | HCID 24758 | — |
| Reactant | N-[2-(Furan-2-yl)-2-oxoethyl]-4-methoxybenzamide | HCID 13773125 | — |
| Product | HCID 13773135 | HCID 13773135 | 73% |
Reaction Steps
11.0 g of N-(4-methoxybenzoyl)-(2-furylcarbonyl)methylamine, 2.0 g of 61% sodium hydride and 7.8 g of ethyl bromoacetate are treated in the same manner ad described in Preparation 1-(2). 10.7 g of ethyl 3-(4-methoxybenzoylamino)-3-(2-furylcarbonyl)propionate are thereby obtained. Yield: 72.8%
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04642313 |
| Source dataset | uspto-grants-1987_02 |
| ORD ID | ord-e36c041459a647d690d9fbad03c56f0d |
| Source note | uspto-grants-1987_02 |