HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 86657498, compound → HCID 58431974, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 86657498 | HCID 86657498 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 58431974 | HCID 58431974 | — |
Reaction Steps
A mixture of 7′-chloro-5-nitro-1,3-dihydrospiro[indene-2,4′-pyrido[2,3-d][1,3]oxazin]-2′(1H)-one from Step A (1.0 g, 3.0 mmol) and 10% palladium on carbon (200 mg) in EtOH (300 mL) is stirred under hydrogen atmosphere for 24 h. The mixture is then filtered through Celite and the filtrate concentrated to give the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08685965B2 |
| Source dataset | uspto-grants-2014_04 |
| ORD ID | ord-31b4766d4db9432e9fe93210416de54e |
| Source note | uspto-grants-2014_04 |