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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2359012Generated: November 1, 2026

HCID 86657498, compound → HCID 58431974, compound

https://huagongshe.com/reaction/2359012

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 86657498HCID 86657498—
CatalystPalladiumHCID 23938—
SolventEthanolHCID 702—
ProductHCID 58431974HCID 58431974—

Reaction Steps

A mixture of 7′-chloro-5-nitro-1,3-dihydrospiro[indene-2,4′-pyrido[2,3-d][1,3]oxazin]-2′(1H)-one from Step A (1.0 g, 3.0 mmol) and 10% palladium on carbon (200 mg) in EtOH (300 mL) is stirred under hydrogen atmosphere for 24 h. The mixture is then filtered through Celite and the filtrate concentrated to give the title compound.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08685965B2
Source datasetuspto-grants-2014_04
ORD IDord-31b4766d4db9432e9fe93210416de54e
Source noteuspto-grants-2014_04