HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethyl bromoacetate → HCID 13773137, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethyl bromoacetate | HCID 7748 | — |
| Reactant | Sodium hydride | HCID 24758 | — |
| Reactant | N-[2-(Furan-2-yl)-2-oxoethyl]-2-methylpropanamide | HCID 13773127 | — |
| Product | HCID 13773137 | HCID 13773137 | 64.2% |
Reaction Steps
13.0 g of N-isobutyryl-(2-furylcarbonyl)methylamine, 3.1 g of 61% sodium hydride and 12.2 g of ethyl bromoacetate are treated in the same manner as described in Preparation 1-(2). 12.0 g of ethyl 3-isobutyrylamino-3-(2-furylcarbonyl)propionate are thereby obtained. Yield: 64.2%
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04642313 |
| Source dataset | uspto-grants-1987_02 |
| ORD ID | ord-bf03fb0af5f543b69128c618eb51726c |
| Source note | uspto-grants-1987_02 |