HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzoyl chloride → N-[2-(Furan-3-yl)-2-oxoethyl]benzamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzoyl chloride | HCID 7412 | — |
| Reactant | Sodium Bicarbonate | HCID 516892 | — |
| Reactant | 2-Amino-1-(furan-3-yl)ethan-1-one--hydrogen chloride (1/1) | HCID 13773121 | — |
| Product | N-[2-(Furan-3-yl)-2-oxoethyl]benzamide | HCID 13773129 | 91.8% |
Reaction Steps
6.0 g of (3-furylcarbonyl)methylamine hydrochloride, 7.8 g of sodium bicarbonate and 5.7 g of benzoyl chloride are treated in the same manner as described in Preparation 1-(1). 7.8 g of N-benzoyl-(3-furylcarbonyl)methylamine are thereby obtained. Yield: 91.8%
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04642313 |
| Source dataset | uspto-grants-1987_02 |
| ORD ID | ord-9c2894dd6ef646048673f0d55cc00d38 |
| Source note | uspto-grants-1987_02 |