Benzoyl chloride, 3,4-dichloro- → 3,4-Dichloro-N-[2-(furan-3-yl)-2-oxoethyl]benzamide

Participants

Role	Name	HCID	Charge
Reactant	Benzoyl chloride, 3,4-dichloro-	HCID 76403	—
Reactant	Sodium Bicarbonate	HCID 516892	—
Reactant	2-Amino-1-(furan-3-yl)ethan-1-one--hydrogen chloride (1/1)	HCID 13773121	—
Product	3,4-Dichloro-N-[2-(furan-3-yl)-2-oxoethyl]benzamide	HCID 13773130	82.4%

Reaction Steps

5.0 g of (3-furylcarbonyl)methylamine hydrochloride, 6.5 g of sodium bicarbonate and 6.8 g of 3,4-dichlorobenzoyl chloride are treated in the same manner as described in Preparation 1-(1). 7.6 g of N-(3,4-dichlorobenzoyl)-(3-furylcarbonyl)methylamine are thereby obtained. Yield: 82.0%

Provenance & Evidence

DOI	10.6084/m9.figshare.5104873.v1
Patent number	US04642313
Source dataset	uspto-grants-1987_02
ORD ID	ord-ded926b3b2c84263897d366be4ffbb66
Source note	uspto-grants-1987_02