HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 58046308, compound → HCID 58046311, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 58046308 | HCID 58046308 | — |
| Solvent | Trifluoroacetic acid | HCID 6422 | — |
| Product | HCID 58046311 | HCID 58046311 | 102.3% |
Reaction Steps
t-butyl-5-chloro-4-(4-chloro-3-(trifluoromethyl)phenoxy)-2-fluorobenzoate (Preparation 50, 245 mg, 0.58 mmol) was dissolved in TFA (4 mL) and the reaction stirred at room temperature for 2 h. The TFA was removed under reduced pressure to give the title compound (219 mg, quant.) as an off-white solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08685977B2 |
| Source dataset | uspto-grants-2014_04 |
| ORD ID | ord-0fb54a8062004d71904c65dd769532a0 |
| Source note | uspto-grants-2014_04 |