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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2359305Generated: November 2, 2026

HCID 58046308, compound → HCID 58046311, compound

https://huagongshe.com/reaction/2359305

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 58046308HCID 58046308—
SolventTrifluoroacetic acidHCID 6422—
ProductHCID 58046311HCID 58046311102.3%

Reaction Steps

t-butyl-5-chloro-4-(4-chloro-3-(trifluoromethyl)phenoxy)-2-fluorobenzoate (Preparation 50, 245 mg, 0.58 mmol) was dissolved in TFA (4 mL) and the reaction stirred at room temperature for 2 h. The TFA was removed under reduced pressure to give the title compound (219 mg, quant.) as an off-white solid.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08685977B2
Source datasetuspto-grants-2014_04
ORD IDord-0fb54a8062004d71904c65dd769532a0
Source noteuspto-grants-2014_04