HuagongsheHuagongshe Chemistry Print Report · For research reference only
Trifluoroacetic acid → HCID 58046335, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Trifluoroacetic acid | HCID 6422 | — |
| Reactant | HCID 58046345 | HCID 58046345 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 58046335 | HCID 58046335 | 100% |
Reaction Steps
Trifluoroacetic acid (1.04 mL, 14 mmol) was added to a mixture of tert-butyl 5-chloro-4-(3,4-dichlorophenylthio)-2-fluorobenzoate (571 mg, 1.40 mmol) in DCM (10 mL) and the reaction stirred at room temperature for 18 hours. The reaction was concentrated to dryness to give the title compound as a white solid (492 mg, 100%). No further purification.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08685977B2 |
| Source dataset | uspto-grants-2014_04 |
| ORD ID | ord-794f6e08535b45a4bba309b993f21723 |
| Source note | uspto-grants-2014_04 |