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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2359331Generated: October 29, 2026

Trifluoroacetic acid → HCID 58046335, compound

https://huagongshe.com/reaction/2359331

Reaction equation

Participants

RoleNameHCIDCharge
ReactantTrifluoroacetic acidHCID 6422—
ReactantHCID 58046345HCID 58046345—
SolventDichloromethaneHCID 6344—
ProductHCID 58046335HCID 58046335100%

Reaction Steps

Trifluoroacetic acid (1.04 mL, 14 mmol) was added to a mixture of tert-butyl 5-chloro-4-(3,4-dichlorophenylthio)-2-fluorobenzoate (571 mg, 1.40 mmol) in DCM (10 mL) and the reaction stirred at room temperature for 18 hours. The reaction was concentrated to dryness to give the title compound as a white solid (492 mg, 100%). No further purification.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08685977B2
Source datasetuspto-grants-2014_04
ORD IDord-794f6e08535b45a4bba309b993f21723
Source noteuspto-grants-2014_04