Back
HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2359353Generated: November 3, 2026

(1,4-Dioxan-2-yl)methanol → HCID 58495831, compound

https://huagongshe.com/reaction/2359353

Reaction equation

Participants

RoleNameHCIDCharge
Reactant(1,4-Dioxan-2-yl)methanolHCID 12655091—
ReactantHCID 58495736HCID 58495736—
ProductHCID 58495831HCID 58495831118.8%

Reaction Steps

Using benzyl 4-(2-{[(4-methylphenyl)sulfony]oxy}ethoxy)piperidine-1-carboxylate (7.8 g, 18.0 mmol) produced in Reference Example 1 (1c) and 1,4-dioxan-2-ylmethanol (1.78 g, 15.1 mmol), the desired title compound (4.4 g, yield 61%) was obtained by the same method as in Reference Examples 1 (1d) and 1 (1e).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08685981B2
Source datasetuspto-grants-2014_04
ORD IDord-130296b72d4341a79296cd6c5d29f0ac
Source noteuspto-grants-2014_04