HuagongsheHuagongshe Chemistry Print Report · For research reference only
(1,4-Dioxan-2-yl)methanol → HCID 58495831, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | (1,4-Dioxan-2-yl)methanol | HCID 12655091 | — |
| Reactant | HCID 58495736 | HCID 58495736 | — |
| Product | HCID 58495831 | HCID 58495831 | 118.8% |
Reaction Steps
Using benzyl 4-(2-{[(4-methylphenyl)sulfony]oxy}ethoxy)piperidine-1-carboxylate (7.8 g, 18.0 mmol) produced in Reference Example 1 (1c) and 1,4-dioxan-2-ylmethanol (1.78 g, 15.1 mmol), the desired title compound (4.4 g, yield 61%) was obtained by the same method as in Reference Examples 1 (1d) and 1 (1e).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08685981B2 |
| Source dataset | uspto-grants-2014_04 |
| ORD ID | ord-130296b72d4341a79296cd6c5d29f0ac |
| Source note | uspto-grants-2014_04 |