HuagongsheHuagongshe Chemistry Print Report · For research reference only
Triphosgene → HCID 58154781, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Triphosgene | HCID 94429 | — |
| Reactant | HCID 58154581 | HCID 58154581 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | HCID 58154781 | HCID 58154781 | — |
Reaction Steps
2-(3-(trifluoromethoxy)phenyl)quinolin-8-amine (252 mg, 0.830 mmol) in toluene (10 mL) was added a mixture of triphosgene (82 mg, 0.275 mmol) in toluene (5 mL). The mixture was stirred for 2 days to obtain 8-isocyanato-2-(3-(trifluoromethoxy)phenyl)quinoline, which was used without isolation.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08685970B2 |
| Source dataset | uspto-grants-2014_04 |
| ORD ID | ord-61e38c84c4524d34ba029dfd53142821 |
| Source note | uspto-grants-2014_04 |