HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 178488919, compound → HCID 178515896, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 178488919 | HCID 178488919 | — |
| Solvent | Acetic Acid | HCID 176 | — |
| Solvent | Hydrogen Bromide | HCID 260 | — |
| Product | HCID 178515896 | HCID 178515896 | 65% |
Reaction Steps
A suspension of 10 (2.6 g, 0.0091 mol) in AcOH (10 ml) and 48% HBr (40 ml) was heated at reflux for 10 hours. After stirring overnight at room temperature the solution was concentrated to dryness and the residue stirred overnight with saturated NaHCO3. The mixture was filtered to yield 1.36 g (65%) of 11.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04642311 |
| Source dataset | uspto-grants-1987_02 |
| ORD ID | ord-1bbd9e9698384e2dbd44f889bc18a800 |
| Source note | uspto-grants-1987_02 |