HuagongsheHuagongshe Chemistry Print Report · For research reference only
Trifluoroacetic acid → HCID 67190686, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Trifluoroacetic acid | HCID 6422 | — |
| Reactant | HCID 67192130 | HCID 67192130 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 67190686 | HCID 67190686 | — |
Reaction Steps
To a solution of Compound 14g (0.78 g; 2.0 mmol) in CH2Cl2 (20 mL) was added TFA (4 mL). The mixture was stirred at room temperature for 4 h. The solvent was evaporated under reduced pressure to afford Compound 14h. The crude product was used in the next reaction without further purification. MS: m/z 290.3 (M+H)+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08685990B2 |
| Source dataset | uspto-grants-2014_04 |
| ORD ID | ord-d4cb3f931ee745588652887e93c4a1e7 |
| Source note | uspto-grants-2014_04 |