Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Ammonia | HCID 222 | — |
| Reactant | HCID 178498875 | HCID 178498875 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 178488972 | HCID 178488972 | 64.4% |
Reaction Steps
A mixture of 63 (21 g, 0.09 mol), CH3OH (700 ml) and NH3 (250 g) was heated in a sealed tube at 120° C. for 24 hours. After washing out the contents, the suspension was concentrated to dryness and the residue crystallized from CH3OH to yield 12.6 g (64%) of 64.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US04642311 |
|---|
| Source dataset | uspto-grants-1987_02 |
|---|
| ORD ID | ord-f3438cbf267044958194867de46ece28 |
|---|
| Source note | uspto-grants-1987_02 |
|---|
