Potassium Hydroxide → HCID 68547606, compound

Participants

Reaction Conditions

Reaction Steps

(2-Aminoquinolin-3-yl)(2,6-dimethoxyphenyl)methanone (0.19 g, 0.6 mmol) was dissolved in diethylene glycol (10 mL), mixed with hydrazine hydrate (0.19 mL, 6.1 mmol) and pulverized potassium hydroxide (0.27 g, 6.7 mmol) and heated for 2 hours at 160° C. The same amounts of hydrazine hydrate and potassium hydroxide were added two more times and the reaction mixture was stirred for two more hours each time at 160° C.

Provenance & Evidence