HuagongsheHuagongshe Chemistry Print Report · For research reference only
Potassium Hydroxide → HCID 68550298, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Potassium Hydroxide | HCID 14797 | — |
| Reactant | Hydrazine hydrate (1:1) | HCID 24654 | — |
| Reactant | HCID 68554149 | HCID 68554149 | — |
| Solvent | Diethylene Glycol | HCID 8117 | — |
| Product | HCID 68550298 | HCID 68550298 | — |
Reaction Conditions
| Temperature | 160 °C |
|---|
Reaction Steps
(2-Amino-6-methoxyquinolin-3-yl)(2-methoxyphenyl)methanone (1.1 g, 3.6 mmol) was dissolved in diethylene glycol (15 mL), mixed with hydrazine hydrate (0.56 mL, 18 mmol) and pulverized potassium hydroxide (1.1 g, 19.8 mmol) and heated to 160° C. for 1.5 hours.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08686002B2 |
| Source dataset | uspto-grants-2014_04 |
| ORD ID | ord-a532f0c16de2430ea9ee216012672185 |
| Source note | uspto-grants-2014_04 |