HuagongsheHuagongshe Chemistry Print Report · For research reference only
1,4-Dioxane → HCID 68550929, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1,4-Dioxane | HCID 31275 | — |
| Reactant | 2-Amino-5-chlorobenzaldehyde | HCID 2773898 | — |
| Reactant | HCID 68550217 | HCID 68550217 | — |
| Solvent | tert-Butanol | HCID 6386 | — |
| Product | HCID 68550929 | HCID 68550929 | — |
Reaction Steps
The title compound was synthesized according to EXAMPLE 11 from 2-amino-5-chlorobenzaldehyde and 3-(2-fluoro-6-methoxyphenyl)propionitrile. Instead of dioxane, tert-butanol was used from [sic; as] the solvent. Reaction time: 5 minutes at 120° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08686002B2 |
| Source dataset | uspto-grants-2014_04 |
| ORD ID | ord-deba9e7f978e4c6da9dd83542bb43299 |
| Source note | uspto-grants-2014_04 |