Carbon Disulfide → HCID 86098808, compound

HRID 2359885Notes

Reaction equation

HRID 2359885 reaction equation
[NH2:1][C:2]1[CH:18]=[CH:17][CH:16]=[CH:15][C:3]=1[CH2:4][NH:5][CH2:6][C:7]1[CH:12]=[CH:11][CH:10]=[CH:9][C:8]=1[O:13][CH3:14].[C:19](=S)=[S:20]>C(O)C>[CH3:14][O:13][C:8]1[CH:9]=[CH:10][CH:11]=[CH:12][C:7]=1[CH2:6][N:5]1[CH2:4][C:3]2[C:2](=[CH:18][CH:17]=[CH:16][CH:15]=2)[NH:1][C:19]1=[S:20]

Participants

4

Reactant 2

HCID 6348Carbon DisulfideHCID 66385424HCID 66385424, compound

Product 1

HCID 86098808HCID 86098808, compound

Reagents, catalysts & solvents 1

HCID 702EthanolSolvent

Procedure

4.0 g (16.51 mmol) (2-aminobenzyl)(2-methoxybenzyl)amine in 100 mL ethanol was mixed with 40 mL CS2 and heated at reflux for 8 hours, forming a yellow precipitate. The mixture was evaluated and the resulting solids were recrystallized in ethanol; 4.24 g white solids.

Workup

  1. temperatureheated
  2. temperatureat reflux for 8 hours
  3. customforming a yellow precipitate
  4. customthe resulting solids were recrystallized in ethanol

Sources & evidence

ORD record
ord-cc12999b4ee548b88ba58166bc43f9b2
Source dataset
uspto-grants-2014_04
Patent number
US08686002B2

Reaction notes

Loading…