HuagongsheHuagongshe Chemistry Print Report · For research reference only
Carbon Disulfide → HCID 86098808, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Carbon Disulfide | HCID 6348 | — |
| Reactant | HCID 66385424 | HCID 66385424 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 86098808 | HCID 86098808 | — |
Reaction Steps
4.0 g (16.51 mmol) (2-aminobenzyl)(2-methoxybenzyl)amine in 100 mL ethanol was mixed with 40 mL CS2 and heated at reflux for 8 hours, forming a yellow precipitate. The mixture was evaluated and the resulting solids were recrystallized in ethanol; 4.24 g white solids.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08686002B2 |
| Source dataset | uspto-grants-2014_04 |
| ORD ID | ord-cc12999b4ee548b88ba58166bc43f9b2 |
| Source note | uspto-grants-2014_04 |