Potassium Carbonate → HCID 66825681, compound
Reaction equation
Cl[C:2]1[N:6]([CH3:7])[N:5]=[C:4]([C:8]([F:11])([F:10])[F:9])[C:3]=1[CH:12]=[O:13].[F:14][C:15]1[CH:16]=[C:17]([OH:22])[CH:18]=[CH:19][C:20]=1[F:21].C(=O)([O-])[O-:24].[K+].[K+]>>[F:14][C:15]1[CH:16]=[C:17]([CH:18]=[CH:19][C:20]=1[F:21])[O:22][C:2]1[N:6]([CH3:7])[N:5]=[C:4]([C:8]([F:11])([F:10])[F:9])[C:3]=1[C:12]([OH:13])=[O:24]Participants
4
Procedure
The title compound was prepared using 5-chloro-1-methyl-3-(trifluoromethyl)-1H-pyrazole-4-carbaldehyde and 3,4-difluorophenol in the manner similar to the method in Production Example 1 above except potassium carbonate was used instead of potassium hydroxide.
Sources & evidence
- ORD record
- ord-4bb8f592c0c64a2d9a73ebdf4f1c8d23
- Source dataset
- uspto-grants-2014_04
- Patent number
- US08686018B2
Reaction notes
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